Trace element analysis techniques

In summary, for determining the sulfur content in a polymer sample that is not soluble in water but is soluble in THF and toluene, an x-ray fluorescence service is recommended as it can be used for a variety of applications and any solubility issues should not be a major concern. Other qualitative tests may require compounds in aqueous solution.
  • #1
ecnerwalc3321
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I have a polymer sample and am interested in qualitatively determining the sulfur (sulfate group) content. Which analytical technique should I consider using? This polymer is not soluble in water but is soluble in THF and toluene. Thanks.
 
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  • #2
Most of the qualitative tests for sulfur that I can recall off the top of my head involve compounds in aqueous solution. Hopefully someone has a better memory than I!

If you have access to an x-ray fluorescence service of some sort, that's probably your best bet, as XRF is used in a variety of applications (polymers, materials, metals, oils), and any solubility issues should not be a huge difficulty. YMMV.
 

FAQ: Trace element analysis techniques

What are trace elements?

Trace elements are chemical elements that are present in very small amounts in a material or substance. They are typically found in concentrations of less than 0.1% by weight.

Why is trace element analysis important?

Trace element analysis is important because trace elements can have a significant impact on the properties and behavior of a material. They can also provide valuable information about the origin and history of a material.

What are some common techniques used for trace element analysis?

Some common techniques used for trace element analysis include atomic absorption spectroscopy (AAS), inductively coupled plasma mass spectrometry (ICP-MS), and X-ray fluorescence (XRF) spectroscopy.

How do these techniques work?

AAS measures the absorption of light by the atoms of a sample to determine the concentration of specific elements. ICP-MS uses high-energy plasma to ionize and atomize a sample, allowing for the detection and quantification of trace elements. XRF spectroscopy measures the fluorescent X-rays emitted by a sample when exposed to high-energy X-rays.

What are some applications of trace element analysis?

Trace element analysis is used in a wide range of fields, including environmental science, geology, forensics, and materials science. It is used to analyze samples such as soil, water, rocks, metals, and biological tissues to understand their composition and identify potential contaminants or sources.

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