- #1
copper-head
- 31
- 8
Hello all.
I have carbonaceous material soaking in Phosphoric acid. I'd like to anneal it under an inert environment to activate the carbon. One method used in literature involved freeze drying the mixture and annealing it as is, as opposed to filtering or centrifuging the mixture. However, I am limited to a regular household freezer and a vacuum chamber. Does anyone have recommendations on how to achieve this with specialty tools?
Cheers
I have carbonaceous material soaking in Phosphoric acid. I'd like to anneal it under an inert environment to activate the carbon. One method used in literature involved freeze drying the mixture and annealing it as is, as opposed to filtering or centrifuging the mixture. However, I am limited to a regular household freezer and a vacuum chamber. Does anyone have recommendations on how to achieve this with specialty tools?
Cheers