Hanging a glass cryostat from a metal support

In summary, the conversation is about hanging a glass cryostat with a bevelled flange at the top. The cryostat stands vertically with the flange angled at 45 degrees. Liquid helium will be used, but lower in the cryostat than the flange. The company quoted for the glass piece does not have an economical solution for hanging it, so the person is hoping to have it made in a local shop. The hanging support is made of cast iron and a piece of foam is needed between the glass and metal. The purpose is to bring the cryostat up and press the o-ring against a flat surface. The person is asking for advice on the best material for the support and if there are any companies
  • #1
swooshfactory
63
0
Hi,

I'm looking to hang a glass cryostat that has a glass bevelled flange at the top. If the cryostat stands vertically, the flange is angled at 45 degrees. Like this (more or less; the silver underscore is just a place holder to get the shape approximately right):

\___/
|__|
|__|

Liquid helium will be put into the cryostat but lower in the cryostat than the flange. The company that has quoted me for the glass piece doesn't have an economical solution to hang it, so I'm hoping to have this made in a shop here.

I believe the hanging support, which is like a collar that encircles the flange and then connects to the rest of our system above it, is made from cast iron. There's also a piece of foam that goes between the glass and the metal, which I'm not sure how to obtain if we have a machine shop here make the cast iron piece (the foam should be ring shaped and sit comfortably in a surface that is angled at 45 degrees).

The idea is that we bring the metal collar up, which brings the cryostat up, and presses the o-ring against a flat surface.

Can anyone offer advice? Is cast iron proper? Is there a company that makes these parts off-the-shelf? The flange won't be custom but rather NW120 or some industry standard. If our machine shop makes the metal support, where can I find this piece of foam and are there any other components I'm missing?


Thanks,
Matt
 
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  • #2
Hi Matt. I take it you have a vacuum insulated, glass cryostat? I've seen them in academia before but they are typically bathed in liquid nitrogen because the latent heat of boiling for LHe is so low. In industry we use a vacuum jacketed and copper shielded, stainless steel container. A conventional vacuum jacketed container used for liquid nitrogen for example, doesn't have sufficient insulating properties.

Should we would assume the ring supporting this is on the outside of the insulation so it won't get cold? In which case, it doesn't much matter what you make it from.
 

FAQ: Hanging a glass cryostat from a metal support

What is a glass cryostat?

A glass cryostat is a scientific instrument used for cooling and maintaining very low temperatures, typically below -100°C. It is primarily used for experiments involving cryogenics, such as studying the properties of materials at extremely low temperatures.

How does a glass cryostat work?

A glass cryostat works by using a combination of insulation and cooling mechanisms to maintain low temperatures. The inner chamber, where the sample is placed, is surrounded by layers of insulation to prevent heat from entering. The outside of the cryostat is connected to a cooling source, such as liquid nitrogen, to keep the temperature stable.

Why is it important to hang a glass cryostat from a metal support?

Hanging a glass cryostat from a metal support is important because it provides stability and prevents the cryostat from moving or vibrating, which could disrupt the experiment. The metal support also helps distribute the weight of the cryostat evenly, reducing the risk of it tipping over.

What materials are suitable for a metal support for a glass cryostat?

The metal support for a glass cryostat should be made of materials that can withstand low temperatures and have good strength and stability. Stainless steel and aluminum are commonly used for cryostat supports, but other metals such as copper and brass may also be suitable.

Are there any safety precautions to consider when hanging a glass cryostat from a metal support?

Yes, there are a few safety precautions to consider when hanging a glass cryostat from a metal support. First, make sure the support is securely attached to a stable surface. Also, be cautious when handling the cryostat and avoid touching any cold surfaces. It is also important to use proper personal protective equipment, such as gloves, when working with cryogenic materials.

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