How to measure average thermal conductivity of a metallic material?

In summary, to measure the average thermal conductivity of a metallic material, one can employ methods such as the guarded hot plate, laser flash analysis, or the transient plane source technique. Each method involves applying a known heat source to the material and measuring the resulting temperature gradient over time. The thermal conductivity is then calculated using Fourier's law of heat conduction, considering factors like sample dimensions, heat flow, and temperature differences. Calibration and adherence to standardized procedures are crucial for accurate results.
  • #1
zenterix
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TL;DR Summary
How exactly does this experiment to measure average thermal conductivity of a metallic slab work?
Heat conduction is the transport of energy between neighboring volume elements in a material as a result of the temperature difference between them.

The "fundamental law of heat conduction", as it is called in the book I am reading, is a "generalization of the results of experiments on the linear flow of heat through a slab perpendicular to the faces".

Pictorially, such experiments do the following

1699738959320.png

The blue rectangular box represents a slab of a material of thickness ##\Delta x## and the area of the side faces is ##A##. One face is maintained at temperature ##T## and the other at ##T+\Delta T##.

The heat that flows perpendicular to the faces for a time ##t## is measured.

The same experiment is repeated by keeping the material the same and varying ##\Delta x## and ##A##.

These experiments lead to the following result

$$\frac{Q}{t} \propto A\frac{\Delta T}{\Delta x}\tag{1}$$

which is approximately true for finite ##\Delta T## and ##\Delta x## and rigorously true when these are infinitesimals.

In this limit, we obtain

$$\frac{dQ}{dt}=-KA\frac{dT}{dx}\tag{2}$$

where the ##dQ## is an inexact differential (I don't know how to write the correct symbol in latex).

The derivative ##dT/dx## is the temperature gradient, ##K## is the thermal conductivity.

My question is about measurement of thermal conductivity.

Here is the experiment for a metal.

The metal is made into the form of a bar, one end is heated electrically, the other end is cooled with a stream of water. The surface of the bar is thermally insulated.

Heat loss through the insulation is calculated by subtracting the rate at which heat enters the water from the rate at which electrical energy is supplied.

The equation used to determine the average thermal conductivity within the given temperature range is

$$K=\frac{L}{A(T_1-T_2)}\frac{dQ}{dt}\tag{3}$$

where again, ##dQ## is an inexact differential.

The temperature difference is measured with thermocouples at two places a distance ##L## apart.

Here is what I think happens

- The amount of heat provided during a certain time to one end of the metal is known (how does one control the amount of heat?). This is ##dQ/dt##.

- ##L## and ##A## are fixed

- The only thing measured is the "temperature difference". This temperature difference seems to be that between the two metallic faces.

However, it also seems that one somehow measures heat entering the water as well. How does one do this?

Does it involve also measuring the temperature difference of the water?
 
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  • #2
zenterix said:
The only thing measured is the "temperature difference". This temperature difference seems to be that between the two metallic faces.
No. The temperature difference is the difference between the readings of the thermocouples that are placed distance ##L## apart. I wouldn't place the thermocouples at the ends of the block where the heat source and sink are because you are likely to get erroneous readings.
zenterix said:
Does it involve also measuring the temperature difference of the water?
Yes, you need to do some calorimetry to find out how much heat enters the water per unit time. The equation for ##K## assumes that no heat is lost as it travels from one end to the other.

Also, you should not record any measurements until you are sure that the steady state is reached. How are you going to figure out when this happens?
 

FAQ: How to measure average thermal conductivity of a metallic material?

What is thermal conductivity and why is it important to measure it in metallic materials?

Thermal conductivity is a measure of a material's ability to conduct heat. It is important to measure it in metallic materials because it affects their performance in applications involving heat transfer, such as in heat exchangers, electronics cooling, and thermal insulation.

What are the common methods used to measure the thermal conductivity of metallic materials?

Common methods include the steady-state method, the transient hot-wire method, and the laser flash method. Each method has its own advantages and is chosen based on the specific requirements of the measurement, such as accuracy, sample size, and temperature range.

How does the steady-state method work for measuring thermal conductivity?

The steady-state method involves establishing a constant temperature gradient across a sample and measuring the heat flow through it. By knowing the heat input and the temperature difference across the sample, the thermal conductivity can be calculated using Fourier's law of heat conduction.

What is the transient hot-wire method and how is it used to measure thermal conductivity?

The transient hot-wire method involves heating a thin wire embedded in the sample with a short electrical pulse and measuring the temperature rise over time. The thermal conductivity is determined by analyzing the temperature response, which depends on how quickly heat is conducted away from the wire.

What is the laser flash method and why is it suitable for metallic materials?

The laser flash method involves subjecting one side of a small, disc-shaped sample to a short laser pulse and measuring the temperature rise on the opposite side. This method is suitable for metallic materials because it is rapid, non-destructive, and can provide accurate measurements over a wide range of temperatures.

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