- #1
bhuwana65
- 7
- 0
Hello ,
We tried to demonstrate preparation of Ammonia by mixing Ammonium Chloride and Calcium Hydroxide in round bottom flask mixed in the proportion of 2:3 .
The flask was in a slanting position with the delivery tube attached to a decicator with Calcium Oxide for drying the gas.
A Flask was attached to the outlet of the decicator for gas collection.
There was no resultant ammonia collected in the collection flask despite a visible flow of gas from the round bottom flask to the decicator on heating.
Need help on identifying the failure of the experiment and suggestions on the rectifications needed to make the experiment sucessful
rgds
Bhuvana
bhuwana65@yahoo.com
We tried to demonstrate preparation of Ammonia by mixing Ammonium Chloride and Calcium Hydroxide in round bottom flask mixed in the proportion of 2:3 .
The flask was in a slanting position with the delivery tube attached to a decicator with Calcium Oxide for drying the gas.
A Flask was attached to the outlet of the decicator for gas collection.
There was no resultant ammonia collected in the collection flask despite a visible flow of gas from the round bottom flask to the decicator on heating.
Need help on identifying the failure of the experiment and suggestions on the rectifications needed to make the experiment sucessful
rgds
Bhuvana
bhuwana65@yahoo.com