How to Identify Phases and Miller Indices in XRD Data?

  • Thread starter anil.bose
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In summary: Hi friends,What is the best way to analyze the XRD data for phase identification and particle size calculation? so far I am using debye-scherrer's formula. Is there any advanced formula?In summary, the best way to analyze XRD data for phase identification and particle size calculation is by using advanced formulas, such as Rietveld Analysis and PANalytical software. It is important to consider factors such as stress-related and instrument-related broadening when calculating particle size, and to have access to a diffractometer and a PDF database. It may also be helpful to seek assistance from experts in the field and to carefully analyze the data using Gaussian fits and error bars.
  • #71
dear friends,
i'm new to XRD and i have some data to analyse..
However, i think that something is wrong with the analysis...could you help me when comparing the results from the pattern of a reference i found in a book...
It has to do with a zeolite material...
I'm desperate!
HELP!
If you want i can provide you with the raw data as they gave me from the lab
 
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  • #72
i have one antimony dross(generated from lead smelting) sample for XRD analysis i have run it but what next how to analyse this data? can somebody help? what phases it is having ?
i am new one in XRD please help.
 
  • #73
pl tell me whether we can get directly the compound existing in an alloy by xrd technique
 
  • #74
hi, could anyone help please ?I have a question ,how to identify miller index in a XRD pattern , I don't have an analysis program,my material is a poly crystal ,and mainly reported to have an orthorohombic and tetragonal structure, it is cu k α (alfa) I also don't know how to identify which 2 theta angel is belongs to which phase of my substance . thanks
 

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